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IN292352: An improved process for the hydrothermal preparation of nickel-zinc ferrite

A new process is developed to recover nickel in the form of a high value product from spent nickel catalyst. The catalyst is treated in chloride media to dissolve nickel and the solution is directly used to prepare nickel-zinc ferrite hydrothermally in ammoniacal medium. The process also avoids additional steps for purification and treatment of leach solution for making intermediate products like nickel salts or metal by evaporation / electrolysis which consumes higher energy. Very uniform nano size Ni-Zn ferrite with high magnetization value of 68.1 emu/g is prepared and reported in this patent. Ni-Zn ferrites are a group of technologically important materials that are used in the fabrication of magnetic, electronic and microwave devices.
Filing Date:
18-11-2009
Issue Date:
30-01-2018
Applicant:
CSIR-National Metallurgical Laboratory (CSIR-NML), Jamshedpur
Patent No:
IN292352
Application No:
2373DEL2009
Inventor(s):
Kamala Kanta Sahu, Archana Agrawal, Devabrata Mishra
IPC Classification:
C07D
Country:
India
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